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4-Acetyl-4'-bromobiphenyl

Product Name
4-Acetyl-4'-bromobiphenyl
CAS No.
5731-01-1
Chemical Name
4-Acetyl-4'-bromobiphenyl
Synonyms
AKOS BAR-2458;TIMTEC-BB SBB005889;Acetylbromodiphenyl;4-ACETYL-4'-BROMODIPHENYL;4-ACETYL-4'-BROMOBIPHENYL;4-Bromo-4'-acetylbiphenyl;4-Acetyl-4'-bromobiphenyl;4-Acetyl-4'-bromobiphenyl 90%;4-(4-BROMOPHENYL)ACETOPHENONE;4-Acetyl-4'-bromobiphenyl >
CBNumber
CB4266556
Molecular Formula
C14H11BrO
Formula Weight
275.14
MOL File
5731-01-1.mol
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4-Acetyl-4'-bromobiphenyl Property

Melting point:
129-133 °C(lit.)
Boiling point:
372.1±17.0 °C(Predicted)
Density 
1.359±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
soluble in Toluene
form 
powder to crystal
color 
White to Orange to Green
BRN 
2048590
InChI
InChI=1S/C14H11BrO/c1-10(16)11-2-4-12(5-3-11)13-6-8-14(15)9-7-13/h2-9H,1H3
InChIKey
UUVKNCRMWPNBNM-UHFFFAOYSA-N
SMILES
C(=O)(C1=CC=C(C2=CC=C(Br)C=C2)C=C1)C
CAS DataBase Reference
5731-01-1(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,N
Risk Statements 
36-51/53
Safety Statements 
26-36-61-24/25-22
RIDADR 
UN 3077 9/PG 3
WGK Germany 
3
HS Code 
2914790090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H319Causes serious eye irritation

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
640468
Product name
4′-(4-Bromophenyl)acetophenone
Purity
97%
Packaging
25g
Price
$84.1
Updated
2024/03/01
Sigma-Aldrich
Product number
640468
Product name
4′-(4-Bromophenyl)acetophenone
Purity
97%
Packaging
100g
Price
$214
Updated
2024/03/01
TCI Chemical
Product number
A1410
Product name
4-Acetyl-4'-bromobiphenyl
Purity
>98.0%(GC)
Packaging
25g
Price
$107
Updated
2024/03/01
Alfa Aesar
Product number
L13798
Product name
4'-(4-Bromophenyl)acetophenone, 97%
Packaging
25g
Price
$65.65
Updated
2024/03/01
Alfa Aesar
Product number
L13798
Product name
4'-(4-Bromophenyl)acetophenone, 97%
Packaging
100g
Price
$189.65
Updated
2024/03/01
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4-Acetyl-4'-bromobiphenyl Chemical Properties,Usage,Production

Chemical Properties

White or pale brown solid

Uses

4-Acetyl-4'-bromobiphenyl is mainly used as a reagent for experimental organic synthesis or reactions, including substitution reactions or the synthesis and polymerisation of biphenyl derivatives.

Synthesis

Dichloromethane was added to Aluminium chloride. The mixture was stirred and cooled to 5 °C in a salt/ice bath. Acetyl chloride was quickly added through a dropping funnel and cooled to ? 3 °C to give a transparent yellow solution. Solid 4-bromobiphenyl was added in small amounts and stirred; wait for ? an hour, then add more. The mixture was stirred for ten hours, rising to 15 °C. The mixture was poured into a bucket of ice /37 percent HCl to destroy the aluminum chloride, then transferred to a separatory funnel and extracted into DCM. Then, the mixture was washed twice with water to destroy HCl. Again, it was washed with 10 percent NaOH and water. The collected DCM layer was dried over magnesium sulfate, mostly filtered by gravity. The solvent was removed in vacuo, and the residue was re-crystallized through ethanol to yield 4-Acetyl-4'-bromobiphen

4-Acetyl-4'-bromobiphenyl Preparation Products And Raw materials

Raw materials

Preparation Products

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4-Acetyl-4'-bromobiphenyl Suppliers

Alchem Pharmtech,Inc.
Tel
8485655694
Email
sales@alchempharmtech.com
Country
United States
ProdList
63711
Advantage
58
Aladdin Scientific
Tel
+1-833-552-7181
Email
sales@aladdinsci.com
Country
United States
ProdList
57511
Advantage
58
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View Lastest Price from 4-Acetyl-4'-bromobiphenyl manufacturers

Career Henan Chemical Co
Product
4-ACETYL-4'-BROMOBIPHENYL 5731-01-1
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
150KG
Release date
2019-07-02

5731-01-1, 4-Acetyl-4'-bromobiphenylRelated Search:


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  • 4-ACETYL-4'-BROMODIPHENYL
  • 4'-(P-BROMOPHENYL)ACETOPHENONE
  • 4'-(4-BROMOPHENYL)ACETOPHENONE
  • 4'-(4-Bromophenyl)acetophenone Synonyms 4-Acetyl-4'-bromobiphenyl
  • TIMTEC-BB SBB005889
  • 4-(4-BROMOPHENYL)ACETOPHENONE
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  • 4-Acetyl-4'-bromobiphenyl &gt
  • Ethanone, 1-(4'-bromo[1,1'-biphenyl]-4-yl)-
  • 4'-(4-Bromophenyl)acetophenyl
  • 4'-(4-Bromophenyl)acetophenyl
  • 4-Acetyl-4'-bromobiphenyl
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  • 5731-01-1
  • 5731-1-1
  • 5371-01-1
  • 5730-01-1
  • ARYL HALIDE
  • Organic Building Blocks
  • Ketones
  • Biphenyls (Building Blocks for Liquid Crystals)
  • Building Blocks for Liquid Crystals
  • Building Blocks
  • Carbonyl Compounds
  • C13 to C14
  • Building Blocks
  • C13 to C14
  • Carbonyl Compounds
  • Chemical Synthesis
  • Organic Building Blocks
  • Aromatic Halides (substituted)
  • C13 to C14
  • Carbonyl Compounds
  • Ketones
  • Biphenyl & Diphenyl ether
  • Electronic Chemicals
  • Bromine Compounds
  • Biphenyls (Building Blocks for Liquid Crystals)
  • Building Blocks for Liquid Crystals
  • Functional Materials
  • 1